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The synthesis and characterization of copper-nickel alloy nanoparticles with a narrow size distribution using sol-gel synthesis
Ferk, Gregor, 1976- ...
Nickel-copper (NiCu) alloy magnetic nanoparticles with a narrow size distribution were prepared by reducing a Ni,Cu-oxide mixture in a silica matrix, obtained with a sol-gel method. In order to ...obtain the NiCu nanoparticles,the silica matrix was treated with an etching solution in an argon atmosphere. By selecting the nominal NiCu alloy composition of 67.5:32.5, a Curie temperature close to 65 1C was achieved. The nanoparticles were superparamagnetic with a magnetization of 8 emu/g at 293 K and exhibited a significant heating ability in an alternating magnetic field. The simplicity of the synthesis allows the preparation of NiCu alloy nanoparticles on a large scale.The method could also be used for the preparation of other mixed-alloy nanoparticles.
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